Isbn: 9798190184860 - handbook of transmission electron microscopy: principles, instrumentation, specimen preparation, imaging, diffraction, spectroscopy, and materials characterization (2 Ergebnisse)

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Taschenbuch. Zustand: Neu. Neuware - Handbook of Transmission Electron Microscopy is a practical and detailed guide to the principles, instruments, methods, and applications of modern TEM. It is written for students, researchers, laboratory scientists, materials engineers, and microscopy professionals who need a clear reference for study, experiment planning, data analysis, and technical reporting. The book begins with electron-specimen interactions, electron optics, microscope architecture, resolution, alignment, and calibration. It then explains specimen preparation for metals, ceramics, semiconductors, powders, thin films, interfaces, polymers, and site-specific FIB samples. Readers will learn how images and diffraction patterns are formed and how to choose suitable methods for a given materials problem. The chapters cover bright-field and dark-field imaging, diffraction contrast, phase contrast, HRTEM, STEM, HAADF imaging, SAED, CBED, nano-beam diffraction, precession electron diffraction, and 4D-STEM. The analytical electron microscopy sections provide clear guidance on: - Energy-dispersive X-ray spectroscopy, including EDS spectra, elemental mapping, peak identification, quantification, and uncertainty- Electron energy-loss spectroscopy, including EELS calibration, low-loss analysis, core-loss edges, ELNES, EFTEM, thickness measurement, and chemical-state interpretation- Electron tomography and three-dimensional reconstruction- Cryo-TEM and low-dose imaging for beam-sensitive materials- In situ and operando TEM for heating, cooling, electrical biasing, mechanical testing, gas-cell work, and liquid-cell studies- Quantitative image analysis, calibration, measurement uncertainty, data integrity, and reproducible workflows>This TEM textbook for materials science also supports work in nanomaterials characterization, microstructure analysis, crystallography, defect analysis, semiconductor research, metallurgy, catalysts, batteries, coatings, and advanced manufacturing materials. The final chapters bring the methods together into complete investigation workflows. They show how to select the right technique, control artefacts, check data quality, interpret results carefully, and prepare professional laboratory reports. Handbook of Transmission Electron Microscopy is suitable for university courses, postgraduate study, laboratory training, independent research, and day-to-day use as a TEM laboratory reference.…