Crystallization of Organic Compounds
Midler Michael Tung Hsien?Hsin McCauley James A. Midler 0Michael Paul Edward L. Tung Hsien-Hsin
ISBN 10: 0471467804 ISBN 13: 9780471467809
Verlag: John Wiley & Sons, 2009
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pp. 300 Illus. Bestandsnummer des Verkäufers 7376904
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Filled with industrial examples emphasizing the practical applications of crystallization methodologies
Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful.
The goal of this text is twofold:
- Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development.
- Improve readers' problem-solving abilities by using actual industrial examples with real process constraints.
With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.
Über die Autorin bzw. den Autor: Hsien-Hsin Tung, PhD, was a senior investigator in Pharmaceutical Research & Development for Merck Research Laboratories until his retirement. Dr. Tung founded the Crystallization Laboratory in Chemical Engineering Research & Development, Merck Research Laboratories.
Edward L. Paul, PhD, is retired director of Chemical Engineering Research & Development at Merck Research Laboratories. In addition to numerous patents and publications, Dr. Paul was coauthor of several chapters in, and senior editor of, the Handbook of Industrial Mixing: Science and Practice (Wiley).
Michael Midler, PhD, is retired senior investigator, Chemical Engineering, with Merck Research Laboratories. His more recent patents and publications are primarily in processes for crystallization and the mixing of liquids. Dr. Midler coauthored, with Dr. Paul, "Mixing in the Fine Chemicals and Pharmaceutical Industries," in the Handbook of Industrial Mixing: Science and Practice.
James A. Mccauley, PhD, was a senior investigator in the Analytical Research Department for Merck Research Laboratories until his retirement. After that, he served as an adjunct professor for the Pharmaceutical Engineering Training Program in the Department of Chemical and Biochemical Engineering at Rutgers University.
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Titel: Crystallization of Organic Compounds
Verlag: John Wiley & Sons
Erscheinungsdatum: 2009
Einband: Hardcover
Zustand: New
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Zustand: New. Hsien-Hsin Tung, PhD, is the co-founder of AcrysPharm, LLC. He founded the crystallization lab. at Merck and center of excellence of particle engineering at AbbVie.Edward L. Paul, PhD, (deceased) was retired Director of Chemical Engineering R & D at Merck R. Artikel-Nr. 812400914
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Buch. Zustand: Neu. Neuware - Crystallization of Organic CompoundsPractical resource covering applications of crystallization principles with methodologies, case studies, and numerous industrial examples for emphasisBased on the authors' hands-on experiences as process engineers, through the use of case studies and examples of crystallization processes, ranging from laboratory development through manufacturing scale-up, Crystallization of Organic Compounds guides readers through the practical applications of crystallization and emphasizes strategies that have proven to be successful, enabling readers to avoid common pitfalls that can render standard procedures unsuccessful.Most chapters feature multiple examples that guide readers, step by step, through the crystallization of active pharmaceutical ingredients (APIs), including an analysis of the major methods of carrying out crystallization operations, their strengths and potential issues, as well as numerous examples of crystallization processes from development through manufacturing scale.Advancements in the field of crystallization have been integrated throughout the book in the newly revised Second Edition to ensure the content adequately reflects current state-of-the-art industrial know-hows and practice. The new edition also adds chapters addressing downstream operations after the crystallization, including filtration/washing and drying, together with industrial use cases.Crystallization of Organic Compounds includes detailed information on:\* Solubility and solid behavior, covering phase rule, polymorph, salt/co-crystal, chiral resolution and in-silico solubility prediction; and kinetics, covering seed, supersaturation, nucleation, crystal growth and model-based experimental design\* Critical issues in the crystallization practice, covering oiling out, seeding/wet-milling, agglomeration/aggregation, mixing scale-up and quality-by-design principles\* Cooling, anti-solvent, evaporation and reactive crystallization process design, covering batch and continuous operations with industrial examples\* Special applications, covering crystallization with ultrasound, reaction selectivity enhancement, and computation fluid dynamics, and solid dispersionWith highly practical coverage of the subject, Crystallization of Organic Compounds is an essential resource for engineers and chemists involved with the development, scaling, or operation of crystallization process in the pharmaceutical and fine chemical industries, particularly those with degrees in chemical engineering and chemistry. Artikel-Nr. 9781119879466
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