NMR Spectroscopy of Polymers places emphasis on the practical use of NMR spectroscopy in polymer chemistry rather than the theoretical treatments. Based on the authors' extensive experimental experience, topics covered include (1) experimental problems such as preparation of sample solution, selection of solvent, internal standard and tube, and contaminants in sample solution, (2) accuracy and precision of NMR measurements required in the analysis of polymer structure such as tacticity, copolymer composition and chain end structures, (3) volume magnetic susceptibility by NMR, (4) stereochemistry of polymer chains, chemical composition and comonomer sequence distribution in copolymers, and end groups and irregular linkages, (5) on-line coupled size exclusion chromatography(SEC) and NMR spectroscopy(SEC/NMR) in which an NMR spectrometer is set in the SEC system as a detector.
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Anbieter: moluna, Greven, Deutschland
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Anbieter: Ria Christie Collections, Uxbridge, Vereinigtes Königreich
Zustand: New. In English. Artikel-Nr. ria9783540402206_new
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Anbieter: AHA-BUCH GmbH, Einbeck, Deutschland
Buch. Zustand: Neu. Druck auf Anfrage Neuware - Printed after ordering - Based on the authors' extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry. This laboratory manual first briefly introduces the basic principles of NMR and considers the key issues of accuracy and precision of the NMR measurements for the analysis of polymer structure such as tacticity, copolymer composition, chain end structures, and volume magnetic susceptibility by NMR. Successive chapters then address stereochemistry of polymer chains, chemical composition and sequence in copolymers, polymerization reactions, two-dimensional NMR spectroscopy, NMR relaxation, and the promising combined use of spectroscopy and chromatography. The book can serve not only as a reference for experienced NMR users but also as an introduction for newcomers. Artikel-Nr. 9783540402206
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